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P323 – 4″ UHV multitech. deposition system NUS

Application

Multi chamber system as combination of UHV MBE system & UHV sputter deposition system for thin film and multilayer deposition at 4″ substrates

Year of delivery

2011

Installation site

National University of Singapore

Design Features

  • Multitechnique deposition system consting a UHV magnetron sputter deposition system and a UHV MBE system connected to a UHV sample preparation chamber.
  • UHV magnetron sputter deposition system with combination of confocal and face to face sputter up configurations.
    • Up to eight 2″ magnetrons in confocal configuration and one 4″ magnetrons in face to face configuration.
      • All 2″ magnetrons mounted at fixed angle.
      • All 2″ magnetrons with easy changeable magnetic system for use with ferromagentic or non-ferromagnetic target materials.
      • DC / Pulsed DC / RF switching unit (two sources connected to one generator).
    • Fully motorized 2 axes sample manipulator with integrated sample shutter and maximal sample temperature above 600°C.
  • UHV MBE system with combination of up to eight effusion cells in confocal configuration and two e-beam sources in face to face configuration.
    • Hot filament effusion cells as well as dual filament effusion cells possible.
    • E-Beam sources as linear multipocket e-beam with motorized pocket exchange.
    • Fully motorized 2 axes sample manipulator with integrated sample shutter and maximal sample temperature well above 800°C.
  • Preperation chamber with moveable magnet setup and ion source.
  • Load lock chamber with storage and lamp heating option.
  • Integrated bake out system.

Special Features

  • RF frequency of 40.68 MHz used for RF sputtering.
  • At least two different sample sizes (4″ and 3″ wafer) can be handled (using different kind of sample holders).

Outer Dimensions

Technical specifications and performance values

General

Sputtering chamber

Size

About 600 mm diameter, about 900 mm height

Material

stainless steel

MBE chamber

Size

About 600 mm diameter, about 930 mm height

Material

stainless steel

Sample preparation chamber

Size

About 400 mm diameter, about 1150 mm height

Material

stainless steel

Load lock chamber

Size

About 250 mm diameter, about 670 mm height

Material

stainless steel

Vacuum

Sputtering chamber

Base pressure

< 10-9 mbar

Pump down time

1.5 hours to < 10-6 mbar

Chamber pumping

Turbo pumping stage in combination with titanium sublimation pumping stage, chamber lid differentially pumped by dry foreline pump

Bake out

< 150°C

MBE chamber

Base pressure

< 7 * 10-11 mbar

Pump down time

2 hours to < 10-6 mbar

Chamber pumping

Turbo pumping stage in combination with titanium sublimation pumping stage, ion getter pumping stage and dry foreline pump

Bake out

< 200°C (inside bake out tent)

Sample preparation chamber

Base pressure

< 5 * 10-9 mbar

Pump down time

1.5 hours to < 2 * 10-6 mbar

Chamber pumping

Turbo pumping stage with dry foreline pump

Bake out

< 120°C

Load lock chamber

Base pressure

< 3 * 10-8 mbar

Pump down time

1 hour to < 5 * 10-6 mbar

Chamber pumping

Turbo pumping stage, chamber door differentially pumped by dry foreline pump

Manipulator features

Sputtering chamber

Sample size

diameter max. 4″ substrate

Motion axes

2 motorized axes (manipulator z translation and (continous) rotation of the sample stage)

Temperatures

Room temperature (not stabilized) up to 600°C at sample

MBE chamber

Sample size

diameter max. 4″ substrate

Motion axes

2 motorized axes (manipulator z translation and (continous) rotation of the sample stage)

Temperatures

Room temperature (not stabilized) up to 1000°C at sample

Sample preparation chamber

Sample size

diameter max. 4″ substrate

Motion axes

2 motorized axes (manipulator z translation and (continous) rotation of the sample stage)

Temperatures

Room temperature (not stabilized) up to 600°C at sample

Sample preparation features

Sample preparation chamber

Ion beam etching /

sample precleaning

Variable ion source to sample distance

Wide range variable ion energy and ion beam current

Plasma treatment

max. 10-3 mbar partly ionised argon gas (using a griddless ion gun)

Load lock chamber

Thermal treatment

max. 180°C at sample (no temperature regulation)

Performance test results

Chamber pump down (part 1)
Chamber pump down (part 2)
Long time sample heating (sputter chamber)
Long time sample heating (sample preparation chamber)
Deposition homogeneity (confocal sputtering)
Magnet performance (Sample preparation chamber)
Deposition homogeneity (face to face sputtering)
RGA at base pressure (MBE chamber)